• Sampling Guidlines

SOIL

Inorganics

Hold TimeAnalysisContainer
28 daysAmmonia4 oz. Glass jar
28 daysChloride4 oz. Glass jar
30 daysChromium, (hexavalent)4 oz. Glass jar
28 daysCOD4 oz. Glass jar
14 daysCyanides4 oz. Glass jar
28 daysFlashpoint4 oz. Glass jar
6 months*Metals, Total4 oz. Glass jar
48 hrNitrate4 oz. Glass jar
48 hrNitrite4 oz. Glass jar
28 daysNitrogen Tot-TKN4 oz. Glass jar
28 daysOil & Grease Or Petroleum HC4 oz. Glass jar
IMMEDPh4 oz. Glass jar
28 daysPhenolics4 oz. Glass jar
28 daysPhosphate Or Phosphorus4 oz. Glass jar
7 daysSolids-Fixed4 oz. Glass jar
7 daysSolids-Total4 oz. Glass jar
7 daysSolids-Volatile4 oz. Glass jar
28 daysSulfate4 oz. Glass jar
7 daysSulfide4 oz. Glass jar
28 daysTOC4 oz. Glass jar
28 daysTX Or EOX4 oz. Glass jar

TCLP

Hold TimeAnalysisContainer
6 months*Metals4 oz. Glass jar
14 (1)Volatiles25 gm ENCORE/4 oz. jar
14 (1)Pesticides4 oz. Glass jar
14 (1)Semi Volatiles4 oz. Glass jar
14 (1)Herbicides4 oz. Glass jar
as aboveFull TCLP (Solid)(1) 25 gm encore and (2) 8 oz. Glass jars

Petroleum Analysis

Hold TimeAnalysisContainer
N/AAge Dating4 Glass jar
14 daysEPH4 oz. Glass jar
14 daysEPH-(MA)4 oz. Amber glass jar
14 daysETPH4 oz. Glass jar
14 daysTPH DRO4 oz. Glass jar
14 daysTPH GRO(2) methanol VOA
28 daysVPH(2) methanol VOA

Organics (Soils/Solids/Oil/Solvents)

Hold TimeAnalysisContainer
3 daysFormaldehyde4 oz. Glass jar
14 daysHerbicides4 oz. Glass jar
14 daysPesticides/PCBs4 oz. Glass jar
14 daysSemi Volatiles4 oz. Glass jar
14 daysVolatiles4 oz. Glass jar, (1) Methanol VOA, (2) Water VOA **
 
(1) 14 Day Hold for TCLP Extraction
(2) 7 Day Hold for TCLP Extraction
***for Method 522, If Chlorinated System, The Preservative Includes Na2so3
**Submit to lab within 48 hours or collection, or freeze
*28 Days For Mercury

WATER

Inorganics

Hold TimeAnalysisPreservativeContainer
14 daysAlkalinityAs Is100 ml/plastic,no headspace
28 daysAmmoniaH2S04 500 ml/plastic
24 hoursBacteria (DW)As Is120 ml/Sterile plastic
6 hoursBacteria (WW)As Is120 ml/Sterile plastic
48 hourBODAs Is500 ml/plastic
28 daysBromideAs Is100 ml/plastic
28 daysChlorideAs Is50 ml/plastic
IMMEDChlorine ResidualAs Is100 ml/plastic
24 hrChromium, HexavalentAs Is250 ml/plastic
28 daysCODH2S0450 ml/plastic
48 hrColorAs Is50 ml/plastic
28 daysConductanceAs Is100 ml/plastic
14 daysCyanideNaOH100 ml/plastic
28 daysFlashpointAs Is250 ml/plastic
28 daysFluoride (ww)As Is 500 ml/plastic
6 monthsHardnessHNO3100 ml/plastic
48 hrMBASAs Is500 ml /plastic
6 months*Metals, Dissolved (Field Filter)HNO3250 ml/plastic
6 months*Metals, Dissolved (Lab Filter)As Is250 ml/plastic
6 months*Metals, Total HNO3 250 ml/plastic
48 hrNitrate, Nitrite As Is50 ml/plastic
28 daysNitrogen, TOT-TKNH2S04250 ml/plastic
24 hrOdor As Is100 ml/plastic
48 hrOdor (NY)As Is250 ml/plastic
28 daysOil & GreaseH2S041000 ml/Amber
IMMEDOxygen, Dissolved As IsBOD Bottle
IMMEDPh As Is100 ml/plastic
28 daysPhenolicsH2S048 oz. Amber
48 hrPhosphate, OrthoAs Is50 ml/plastic
28 daysPhosphate, PhosphorusH2S0450 ml/plastic
7 daysSolids, Dissolved As Is100 ml/plastic
48 hrSolids, SettleableAs Is1000 ml/plastic
7 daysSolids, SuspendedAs Is100 ml/plastic
7 daysSolids, Total As Is100 ml/plastic
7 daysSolids, VolatileAs Is100 ml/plastic
28 daysSulfateAs Is50 ml/plastic
7 daysSulfideNaOH/Zinc Acetate 250 ml/plastic
IMMEDSulfiteAs Is100 ml/plastic
28 daysTOCH3PO48 oz. Amber
28 daysTOXH2S04250 ml/Amber
48 hrTurbidity As Is100 ml/plastic
48 hrUV 254As Is8 oz. Amber
14 daysVolatile Fatty AcidsAs Is or H2SO4250 ml plastic or glass

TCLP

Hold TimeAnalysisPreservativeContainer
6 months*Metals As Is500 ml plastic
14 days (1)VolatilesAs Is(4)-40 ml/VOA Vials
7 days (2)Semi VolatilesAs Is1000 ml/Amber
7 days (2)PesticidesAs Is1000 ml/Amber
7 days (2)HerbicidesAs Is1000 ml/Amber
as aboveFull TCLP (Liquid)As Is(3) 1000 ml glass Ambers, (1) 500 ml plastic,(4) 40 ml VOA Vials

Petroleum Analysis

Hold TimeAnalysisPreservativeContainer
14 daysEPHHCL(2) 1000 ml/Amber
7 daysETPHAs Is1000 ml/Amber
7 daysTPH DROAs Is1000 ml/Amber
14 daysTPH GROHCL(2)-40 ml/VOA Vials
14 daysVPHHCL(2)-40 ml/VOA Vials

Organics (Liquids)

Hold TimeAnalysisPreservativeContainer
14 days1,4 Dioxane by method 8260HCL(3)-40ml VOA Vials
28 days1,4 Dioxane Low Level 8270 Or 522***NAHSO48 oz. Amber
14 daysAlcoholsAs Is(2)-40 ml VOA Vials
14 daysDissolved Gasses HCL(3)-40 ml/VOA Vials
14 daysEDB/DBCPAs Is(2)-40 ml VOA Vials
3 daysFormaldehydeAs Is8 oz. Amber
14 daysGlycolsAs Is(2)-40 ml VOA Vials
14 daysHaloacetic Acids (HAA5)NH4CL4 oz. Amber
7 daysHerbicidesAs Is1000 ml/Amber
14 daysOxygenatesTSP(3)-40 ml VOA Vials
7 daysPCBsAs Is1000 ml/Amber
7 daysPesticidesAs Is1000 ml/Amber
7 daysSemi Volatiles As Is(2) 1000 ml/Amber
14 daysTHMsNa2S2O3(3)-40 ml/VOA Vials
14 daysVolatiles HCL(3)-40 ml VOA Vials
14 days / 3 daysVolatiles (624) HCL / As isHCL / As Is(3)-40 ml VOA Vials / (2)-40 ml VOA Vials As Is
 
(1) 14 Day Hold for TCLP Extraction
(2) 7 Day Hold for TCLP Extraction
***for Method 522, If Chlorinated System, The Preservative Includes Na2so3
**Submit to lab within 48 hours or collection, or freeze
*28 Days For Mercury